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Immediately before the start of the NMR measurements, 1.0 mL of the different 10% D 2 O-containing samples was added to the Eppendorf tube, of which 0.5 mL was transferred to a 5 mm NMR tube, which was then closed with a polyethylene cap
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Proceedings of the National Academy of Sciences of the United States of America 112 (2015) 14960–5
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